Green S.O.C.

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      group 06 11 2015

Laboratory of Green Synthetic Organic Chemistry

 contacts publications

  GROUP LEADER:  Prof. Luigi Vaccaro   

 

 

GROUP members

  

RECENT NEWS  


Newly accepted publications at Green SOC:

 

VERY IMPORTANT Heterogeneous C–H Alkenylations in Continuous-Flow: Oxidative Palladium-Catalysis in a Biomass-Derived Reaction Medium,

Green Chem., 2017, in press 10.1039/C7GC01103B.

 

Biomass-derived solvents as effective media for cross-coupling reactions and C–H functionalization processes

Has been selected among the 2017 Green Chemistry Hot Articles, congratulations !!!
Green Chem. 2017,19,1601-1612.

 

J. Pina, D. Santos
Sarmento, M. Accoto, P. L. Gentili, A. M. Galvão, Luigi Vaccaro*, J. S. Seixas de Melo*, Excited State Proton Transfer in Indigo, J. Phys.
Chem. B, J. Phys. Chem. B, 2017, 121, 2308–2318.

D. Lanari, O. Piermatti, C. Morozzi, S. Santoro, L. Vaccaro*, Recent Applications of Solid-Supported Ammonium Fluorides in Organic Synthesis,  Synthesis 2017, 49, 973-980.
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Congratulations to Chiara who just defended her PhD thesis with a excellent presentation of her work 

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November 2016, Lorenzo and Federica started the PhD course at Green SOC, good luck !!!
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In celebration of Peer-Review Week, Luigi has been selected among the top 10 reviewers in 2016 by the editor of Green Chemistry for his significant contribution to the journal.

Considering our reserach field and the preminent role of this journal in the development of Green Chemistry, this recognition is particularly appreciated.
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H-CCAT project has been fully financed by EU Commision within the call NMBP 01-2016: Novel hybrid materials for heterogeneous catalysis. Among the many activities, Green SOC will be leading WP3 on "Catalytic Testing and Design of New Catalytic Sites".
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Newly accepted publications at Green SOC:

- NEW ON furfuryl alcohol azeotrope!!! Searching for novel reusable biomass-derived solvents: furfuryl alcohol/water azeotrope as medium for the waste-minimised copper-catalysed azide-alkyne cycloaddition, Green Chem. DOI: 10.1039/C6GC01941B

Sustainable Approach to Waste-Minimized Sonogashira Cross-Coupling Reaction Based on Recoverable/Reusable Heterogeneous Catalytic/Base System and Acetonitrile Azeotrope, ACS Sus. Chem. Eng. DOI: 10.1021/acssuschemeng.6b02170

-Click-Chemistry Approaches to Pi-conjuganted polymers for organic electronics applications Chemical Science 2016 in press DOI: 10.1039/C6SC01832G

- Selective monomethyl esterification of linear dicarboxylic acids with bifunctional alumina catalysts, Green Chem. DOI: 10.1039/C6GC01900E


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Luigi has been invited to give a Keynote lecture at 2016 International IUPAC Conference on Green Chemistry and at THe university of Stockholm
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Our contribution G. Strappaveccia, S. Ziarelli, F. Pizzo, L. Vaccaro*. PS-BEMP as a Heterogeneous Base Catalyst for Phospha-Michael Addition of α,β-Unsaturated Ketones. Org. Biomol. Chem. 2016, 14, 35213525. has been highlighted in Synfacts 201612 (07), 0759

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Newly accepted publications at Green SOC:

-Current synthetic tools for the preparation of semiconducting polymers. Energy Environ. Sci., 2016, 9 , 763‒786.

- A Catalytic Peterson-like Synthesis of Alkenyl Nitriles. Org. Lett. DOI: 10.1021/acs.orglett.6b01121

 A Protocol for the Waste-Minimized Synthesis of β-Cyano Ketones Promoted by a Heterogeneous Fluoride Catalyst. Adv. Synth.Catal. 2016, in press, DOI:10.1002/adsc.201600287

HIGHLIGHTED in Synfacts 2016 12, 11, 1101. DOI: 10.1055/s-0036-1589222

- In collaboration with Lutz Ackermann: Heterogeneous Catalytic Approaches in C–H Activation Reactions. Green Chem., 2016, DOI:10.1039/C6GC00385K
- Heterogeneous Palladium-Catalysed Catellani Reaction in Biomass-Derived γ-Valerolactone, Green Chem., 2016, DOI:10.1039/C6GC01393G 
X. Tian, F. Yang, D. Rasina, S. Warratz, M. Bauer, F. Ferlin. L. Vaccaro*,  L. Ackermann*. C–H Arylations of 1,2,3-Triazoles by Reusable Heterogeneous Palladium Catalysts in Biomass-Derived γ-Valerolactone, Green Chem. 2016in press,DOI: 10.1039/C6CC03468C  

 

          NEWS       contactspublications       



 

 Research overview                                    VIEW HERE FOR RECENT SELECTED EXAMPLES

 

 

NEW POLYMERS FOR IMMOBILIZED CATALYTIC SYSTEMS FOR SUSTAINABLE CATALYSIS IN FLOW
CLICK to view larger                                 

 

 

 

 

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Domino Hydrogenation−Reductive Amination of Phenols, a Simple Process To Access Substituted Cyclohexylamines
Org. Lett. 2015, 17, 3990−3993   DOI: 10.1021/acs.orglett.5b01842

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Eur. Pol. J.2015,73, 391–401   DOI: 10.1016/j.eurpolymj.2015.10.002

RSC Advances, 2015, 5, 107200 - 107208   DOI: 10.1039/c5ra21140a


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Accessing stable zirconium carboxyaminophosphonate nanosheets as support for highly active Pd nanoparticlesChem. Commun., 2015, 51, 15990--15993   DOI: 10.1039/c5cc06292f

 


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Aquivion PFSA as a Novel Solid and Reusable Acid Catalyst in the Synthesis of 2‑Pyrrolidin-2-ones in Flow
ACS Sustainable Chem. Eng. 2015, 3, 1873−1880  DOI: 10.1021/acssuschemeng.5b00470

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Green Chem. 201517, 365‑372 DOI: 10.1039/C4GC01677G
Biomass-derived safe medium to replace toxic dipolar solvents and access cleaner Heck coupling reactions.

Green Chem. 201517, 1071‑1076 DOI: 10.1039/c4gc01728e
γ-Valerolactone as an alternative biomass-derived medium for the Sonogashira reactionreactions.

ACS Sustainable Chem. Eng. 2014, 2, 2461−2464 dx.doi.org/10.1021/sc5004727
γ‑Valerolactone as a Renewable Dipolar Aprotic Solvent Deriving from Biomass Degradation for the Hiyama Reaction.

 

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Org. Process Res. Dev. in press  DOI: 10.1021/acs.oprd.5b00163 
An Efficient and Waste-Minimized One-Pot Procedure for the Preparation of γ‑Amino Alcohols Starting from α,β-Unsaturated Ketones in Flow.


 

 

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